Monodisperse sphere-on-sphere silica particles for fast HPLC separation of peptides and proteins.
نویسندگان
چکیده
Monodisperse sphere-on-sphere (SOS) silica particles are produced in a one-pot reaction, removing the need for time-consuming preparation and classification steps. Analysis of peptides and proteins using HPLC displays faster separation at lower operating pressure than commercially available fused core materials.
منابع مشابه
Multi-step Coating of Monodisperse Silica Spheres by Titania Nanoparticles Base on Electrostatic Attraction Strategy
TiO2-SiO2 core-shell particles include of monodisperse silica core and nanostructured titania shell were synthesized by a multi-step coating process. The monodisperse silica spheres were synthesized by Stöber method and titania shell was obtained of a colloidal sol prepared by a hydrolysis–condensation reaction. The titania sol was deposited on monodisperse silica spheres by a multi-step coatin...
متن کاملExperimental observation of the crystallization of hard-sphere colloidal particles by sedimentation onto flat and patterned surfaces.
We present a confocal microscopy study of 1.55 microm monodisperse silica hard spheres as they sediment and crystallize at the bottom wall of a container. If the particles sediment onto a feature less flat wall, the two bottom layers crystallize simultaneously and layerwise growth follows. If the wall is replaced by a hexagonal template, only layerwise growth occurs. Our results complement earl...
متن کاملAdaptive neuro-fuzzy inference system and neural network in predicting the size of monodisperse silica and process optimization via simulated annealing algorithm
In this study, Back-propagation neural network (BPNN) and adaptive neuro-fuzzy inference system (ANFIS) methods were applied to estimate the particle size of silica prepared by sol-gel technique. Simulated annealing algorithm (SAA) employed to determine the optimum practical parameters of the silica production. Accordingly, the process parameters, i.e. tetraethyl orthosilicate (TEOS), H2O and N...
متن کاملNon-Fourier heat conduction equation in a sphere; comparison of variational method and inverse Laplace transformation with exact solution
Small scale thermal devices, such as micro heater, have led researchers to consider more accurate models of heat in thermal systems. Moreover, biological applications of heat transfer such as simulation of temperature field in laser surgery is another pathway which urges us to re-examine thermal systems with modern ones. Non-Fourier heat transfer overcomes some shortcomings of Fourier heat tran...
متن کاملA Numerical Study on Agglomeration in High Temperature Fluidized beds
Soft-sphere discrete element method (DEM) and Navier-Stokes equations were coupled with equations of energy for gas and solids to investigate the process of agglomeration in fluidized bed of polyethylene particles at high temperature. The Newton’s second law of motion was adapted for translational and rotational motion of particles and agglomerates. The cohesive force for polyethylene particles...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
عنوان ژورنال:
- The Analyst
دوره 139 22 شماره
صفحات -
تاریخ انتشار 2014